Synthesis of Pristine Al2O3 Powder Via Self-Propagating Combustion Method with Various Fuel Sources

Authors

  • Missha Balqis Shariamin Faculty of Applied Sciences, Blok C, Kompleks Sains 2, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Mas Fiza Mustafa Faculty of Applied Sciences, Blok C, Kompleks Sains 2, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Mohd Sufri Mastuli Faculty of Applied Sciences, Blok C, Kompleks Sains 2, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia; Institute of Science, Level 3, Kompleks Inspirasi, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
  • Annie Maria Mahat Faculty of Applied Sciences, Blok C, Kompleks Sains 2, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia; Institute of Science, Level 3, Kompleks Inspirasi, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia

DOI:

https://doi.org/10.24191/scl.v18i2.6549

Keywords:

Al2O3, Structural, Oxidation, Thermal analysis, X-ray techniques

Abstract

In this study, pristine Al2O3 powder was prepared by a simple self-propagating combustion (SPC) method. The effect of the different fuels on synthesized Al2O3 powder on thermal, structural, and morphological properties was investigated. The fuels utilized include formic, citric, oxalic, and tartaric acids. Based on the STA results, all precursors were annealed at 1100ºC for 24 hours to obtain pristine Al2O3 powder. XRD results show that all samples correspond to the α-Al2O3 crystal structure. Notably, differences in the morphology and particle size of all samples were observed through FESEM micrographs.

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Published

2024-06-24

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